GB/T 23356-2024 卷烟 烟气气相中一氧化碳的测定 非散射红外法

GB/T 23356-2024 Cigarettes—Determination of carbon monoxide in the vapour phase of cigarette smoke—NDIR method

国家标准 中文简体 即将实施 页数:16页 | 格式:PDF

基本信息

标准号
GB/T 23356-2024
标准类型
国家标准
标准状态
即将实施
中国标准分类号(CCS)
国际标准分类号(ICS)
发布日期
2024-10-26
实施日期
2025-05-01
发布单位/组织
国家市场监督管理总局、国家标准化管理委员会
归口单位
全国烟草标准化技术委员会(SAC/TC 144)
适用范围
本文件描述了卷烟烟气气相中一氧化碳的非散射红外测定方法。
本文件适用于卷烟烟气气相中一氧化碳的测定。

文前页预览

研制信息

起草单位:
国家烟草质量监督检验中心、中国烟草标准化研究中心、中国烟草总公司郑州烟草研究院、河南中烟工业有限责任公司、云南中烟工业有限责任公司、河北中烟工业有限责任公司、上海市烟草质量监督检测站、福建中烟工业有限责任公司、广西中烟工业有限责任公司、广东中烟工业有限责任公司、贵州中烟工业有限责任公司、江苏中烟工业有限责任公司、重庆中烟工业有限责任公司、甘肃烟草工业有限责任公司
起草人:
庞永强、陈志浩、李翔宇、叶长文、姜兴益、陈宸、罗彦波、张宇、田海英、何爱民、陈云璨、秦亚琼、刘巍、余晶晶、刘德祥、刘泽春、姬厚伟、鹿洪亮、郝红玲、翟玉俊、秦艳华、韶济民、张杰、张玉璞、王娟、朱先约、倪建彬、吴永良、蔡洁云、李倩、游金清、马丽娜、田大勇、郑捷琼、丁丽、曹常伟、孙海峰、吕晓东、尚军、焦玲玲、王勇、楚文娟、王龙、许蔼飞、彭春鸣、班晓瑞
出版信息:
页数:16页 | 字数:15 千字 | 开本: 大16开

内容描述

ICS65.160

CCSX87

中华人民共和国国家标准

GB/T23356—2024

代替GB/T23356—2009

卷烟烟气气相中一氧化碳的测定

非散射红外法

Cigarettes—Determinationofcarbonmonoxideinthevapourphaseof

cigarettesmoke—NDIRmethod

(ISO8454:2024,MOD)

2024⁃10⁃26发布2025⁃05⁃01实施

国家市场监督管理总局

国家标准化管理委员会发布

GB/T23356—2024

目次

前言··························································································································Ⅲ

1范围·······················································································································1

2规范性引用文件········································································································1

3术语和定义··············································································································1

4原理·······················································································································1

5试剂或材料··············································································································1

6仪器设备·················································································································2

7分析步骤·················································································································2

7.1抽吸卷烟的准备··································································································2

7.2调节·················································································································2

7.3非散射红外分析仪校准·························································································2

7.4吸烟与气相捕集··································································································3

7.5一氧化碳体积浓度测定·························································································3

8试验数据处理···········································································································3

8.1计算每支卷烟烟气一氧化碳的平均体积····································································3

8.2计算每支卷烟一氧化碳的平均质量··········································································3

9重复性和再现性········································································································4

10测试报告···············································································································4

10.1通则················································································································4

10.2卷烟的唯一性资料······························································································4

10.3采样信息··········································································································4

10.4测试说明··········································································································4

10.5测试结果··········································································································5

附录A(资料性)方法的重复性限和再现性限·····································································6

GB/T23356—2024

前言

本文件按照GB/T1.1—2020《标准化工作导则第1部分:标准化文件的结构和起草规则》的规

定起草。

本文件代替GB/T23356—2009《卷烟烟气气相中一氧化碳的测定非散射红外法》,与GB/T23356—

2009相比,除结构调整和编辑性改动外,主要技术变化如下:

——更改了收集气袋的容积规定(见6.3,2009年版的5.3);

——更改了非散射红外分析仪采样速率的规定(见6.4,2009年版的5.4);

——更改了温度计的精度要求(见6.8,2009年版的5.7);

——更改了一氧化碳标准气体浓度(见第5章、7.3.2和7.3.5,2009年版的第6章、8.2.2和8.2.5);

——删除了抽样的规定(见2009年版的第7章);

——更改了卷烟抽吸的规定(见7.4.2,2009年版的8.3.2);

——增加了非散射红外分析仪重新校准的要求(见7.5.1)。

本文件修改采用ISO8454:2024《卷烟烟气气相中一氧化碳的测定非散射红外法》。

本文件与ISO8454:2024相比做了下述结构调整:

——第5章对应ISO8454:2024的第6章;

——第6章对应ISO8454:2024的第5章;

——增加了7.1,第7章中其他条号顺延;

——10.1对应ISO8454:2024的第10章;

——增加了附录A。

本文件与ISO8454:2024的技术差异及其原因如下:

——用规范性引用的GB/T16447替换了ISO3402、GB/T16450替换了ISO3308、GB/T19609

替换了ISO4387,引用相应的国家标准,便于对本文件的理解和执行;

——更改了ISO8454:2024中重复性和再现性相关内容(见第9章),以适合国内现状;

——增加了抽吸卷烟的准备相关内容(见7.1),以适合我国国情便于标准的操作和执行;

——增加了标准条件下每支卷烟一氧化碳的平均质量的计算公式[见公式(3)],便于在标准条件

下进行快速计算;

——增加了测试报告的详细内容(见10.2~10.5),适合我国国情便于标准的操作和执行。

本文件做了下列编辑性改动:

——增加了资料性附录A“方法的重复性限和再现性限”。

请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。

本文件由国家烟草专卖局提出。

本文件由全国烟草标准化技术委员会(SAC/TC144)归口。

本文件起草单位:国家烟草质量监督检验中心、中国烟草标准化研究中心、中国烟草总公司郑州烟

草研究院、河南中烟工业有限责任公司、云南中烟工业有限责任公司、河北中烟工业有限责任公司、上

海市烟草质量监督检测站、福建中烟工业有限责任公司、广西中烟工业有限责任公司、广东中烟工业有

限责任公司、贵州中烟工业有限责任公司、江苏中烟工业有限责任公司、重庆中烟工业有限责任公司、

甘肃烟草工业有限责任公司。

本文件主要起草人:庞永强、陈志浩、李翔宇、叶长文、姜兴益、陈宸、罗彦波、张宇、田海英、何爱民、

陈云璨、秦亚琼、刘巍、余晶晶、刘德祥、刘泽春、姬厚伟、鹿洪亮、郝红玲、翟玉俊、秦艳华、韶济民、张杰、

GB/T23356—2024

张玉璞、王娟、朱先约、倪建彬、吴永良、蔡洁云、李倩、游金清、马丽娜、田大勇、郑捷琼、丁丽、曹常伟、

孙海峰、吕晓东、尚军、焦玲玲、王勇、楚文娟、王龙、许蔼飞、彭春鸣、班晓瑞。

本文件及其所代替文件的历次版本发布情况为:

——2009年首次发布为GB/T23356—2009;

——本次为第一次修订。

GB/T23356—2024

卷烟烟气气相中一氧化碳的测定

非散射红外法

1范围

本文件描述了卷烟烟气气相中一氧化碳的非散射红外测定方法。

本文件适用于卷烟烟气气相中一氧化碳的测定。

2规范性引用文件

下列文件中的内容通过文中的规范性引用而构成本文件必不可少的条款。其中,注日期的引用文

件,仅该日期对应的版本适用于本文件;不注日期的引用文件,其最新版本(包括所有的修改单)适用于

本文件。

GB/T16447烟草及烟草制品调节和测试的大气环境(GB/T16447—2004,ISO3402:1999,

IDT)

GB/T16450常规分析用吸烟机定义和标准条件(GB/T16450—2004,ISO3308:2000,

MOD)

GB/T19609卷烟用常规分析用吸烟机测定总粒相物和焦油(GB/T19609—2024,ISO4387:

2019,MOD)

3术语和定义

下列术语和定义适用于本文件。

3.1

气相vapourphase

使用符合GB/T16450要求的吸烟机,按GB/T19609抽吸卷烟过程中通过烟气捕集器的烟气

部分。

3.2

清除抽吸clearingpuff

熄灭卷烟后或从卷烟夹持器上取下卷烟后进行的任何抽吸。

4原理

按GB/T19609抽吸卷烟,收集卷烟烟气气相,用非散射红外分析仪测定一氧化碳,计算出每支卷

烟烟气中一氧化碳量。

5试剂或材料

采用有效期内纯度不低于99.999%的氮气作为一氧化碳标准气体的混合气。非散射红外分析仪

应用至少三种相对误差小于2%的已知浓度标准气体进行校准,标准气体浓度范围应覆盖预期检测到

的一氧化碳浓度,以免外推曲线。宜采用一氧化碳浓度(体积分数)为1%、3%和5%的标准气体。

1

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