GB/T 44202-2024 馆藏丝织品老化程度测试样品制备

ICS

97.195；19.020

CCS

Y04

中华人民共和国国家标准

GB/T44202—2024

馆藏丝织品老化程度测试样品制备

Samplepreparationfortestingagingdegreeofsilktextileinmuseumcollections

2024-07-24发布2024-11-01实施

国家市场监督管理总局发布

国家标准化管理委员会

GB/T44202—2024

目次

前言

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1

范围

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2

规范性引用文件

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3

术语和定义

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4

取样

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4.1

取样计划

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4.2

取样过程

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5

样品处理

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5.1

样品清洗

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5.2

样品调湿

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6

样品制备

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7

样品信息登记

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附录A（资料性）

馆藏丝织品取样信息记录表样式

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附录B（资料性）

馆藏丝织品老化程度测试样品信息表样式

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参考文献

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Ⅰ

GB/T44202—2024

前言

本文件按照GB/T1.1—2020《标准化工作导则第1部分：标准化文件的结构和起草规则》的规定

起草。

请注意本文件的某些内容可能涉及专利。本文件的发布机构不承担识别专利的责任。

本文件由中华人民共和国国家文物局提出。

本文件由全国文物保护标准化技术委员会（SAC/TC289）归口。

本文件起草单位：中国科学技术大学、中国国家博物馆、福建理工大学、北京中科标准科技集团有

限公司。

本文件主要起草人：龚钰轩、龚德才、铁付德、王志民、成维智、周光昭、乔成全、胡霜晴、

钟博超、张晓宁、王开、罗贤娟。

Ⅲ

GB/T44202—2024

馆藏丝织品老化程度测试样品制备

1范围

本文件规定了馆藏丝织品老化程度测试样品的取样、处理、制备、样品信息登记等要求。

本文件适用于馆藏丝织品老化程度分析中氨基酸分析、扫描电子显微镜、热重分析、傅里叶变换红

外光谱、X射线粉末衍射测试方法的样品制备。

2规范性引用文件

下列文件中的内容通过文中的规范性引用而构成本文件必不可少的条款。其中，注日期的引用文

件，仅该日期对应的版本适用于本文件；不注日期的引用文件，其最新版本（包括所有的修改单）适用

于本文件。

GB/T6529—2008纺织品调湿和试验用标准大气

GB/T13464—2008物质热稳定性的热分析试验方法

GB/T23863—2009博物馆照明设计规范

GB/T32016—2015蚕丝氨基酸的测定

JGJ66—2015博物馆建筑设计规范

3术语和定义

GB/T6529—2008界定的以及下列术语和定义适用于本文件。

3.1

丝织品老化程度agingdegreeofsilktextile

与新鲜蚕丝相比，馆藏丝织品受损后所产生的微观结构和宏观性能变化的水平。

4取样

4.1取样计划

馆藏丝织品老化程度测试样品（以下简称“样品”，包括待测样品和参比样品1））制备应与文物的

负责单位协商后根据取样目的制定取样计划，取样计划的相关要求如下：

a）应充分考虑历次保护修复使用的材料和工艺对测试产生的影响；

b）根据需要和文物等级、保存状况、病害、组织结构等特点，确定取样位置、取样数量、取样量

（如样品尺寸、样品面积和样品质量）、取样方法、样品包装和保存方法等；

c）优先从残件（片）或对文物价值信息（如花纹、图案等）影响较小的地方取样；

d）确定样品测试后剩余样品的处置方式（如归还原文物负责单位、自己留存等）。

4.2取样过程

取样过程根据取样计划进行。

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1）参比样品为用于分析比较的，与待测样品采取相同准备、制作、测试的新样品。

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